HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one → 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 10353298 | — |
| Edukt | N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide | HCID 12119265 | — |
| Produkt | 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 22449453 | — |
Reaktionsschritte
The reaction was carried out in the same manner as in Example 1-(2), except that 270 mg of the compound prepared in (2) above was used instead of 8-acetylamino-1-tetralone of Example 1-(2). The reaction mixture obtained by the post-treatment was further reacted in the same manner as in Example 1-(3) and post-treated to produce 126 mg of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05834476 |
| Quelldatensatz | uspto-grants-1998_11 |
| ORD ID | ord-a6c9eea160d542618b7334d21eca165d |
| Quellennotiz | uspto-grants-1998_11 |