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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 356284Erstellt: 24. Oktober 2026

Methyl (4-nitrophenoxy)acetate → Methyl(4-aminophenoxy)acetate

https://huagongshe.com/de/reaction/356284

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl (4-nitrophenoxy)acetateHCID 700522—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
ProduktMethyl(4-aminophenoxy)acetateHCID 642211597,6%

Reaktionsschritte

A procedure similar to that described in Example 6 was repeated, except that 30.8 g of methyl 4-nitro-phenoxyacetate (prepared as described in Preparation 36), 5.0 g of 10% w/w palladium-on-charcoal and 500 ml of methanol were used, to give 25.8 g of the title compound having Rf=0.79 (on silica gel thin layer chromatography using ethyl acetate as the developing solvent).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05834501
Quelldatensatzuspto-grants-1998_11
ORD IDord-d75c053e7dda43a784c033be9ddf82c9
Quellennotizuspto-grants-1998_11