HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Octylaniline → N-(p-octylphenyl)-2,4,6-triphenylpyridinium triflate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Octylaniline | HCID 85346 | — |
| Edukt | AG-G-77560 | HCID 2778031 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N-(p-octylphenyl)-2,4,6-triphenylpyridinium triflate | HCID 20064818 | — |
Reaktionsschritte
A 4.58-g portion (0.01 mole) of 2,4,6-triphenylpyrylium triflate is added to 200 ml of ethanol. To this solution, 2.05 g (0.01 mole) of p-n-octylaniline is added. The mixture is refluxed for about 20 hours. Upon removing the ethanol by rotating evaporation, an orange oil remains. To remove the last of the ethanol the oil is placed under high vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05000873 |
| Quelldatensatz | uspto-grants-1991_03 |
| ORD ID | ord-7852d11320734bafb0ba94ae0caa2fb1 |
| Quellennotiz | uspto-grants-1991_03 |