Benzoyl isothiocyanate → 2-[[(Benzoylamino)thioxomethyl)amino]-5-methylbenzamide

Beteiligte Stoffe

Reaktionsschritte

To a stirred mixture of 4.5 g of 2-amino-5-methylbenzamide and 200 ml of ether was added dropwise, a solution of 4.9 g benzoyl isothiocyanate in 100 ml of ether over 20 minutes. After stirring overnight, the solid was collected, giving 8.7 g of the desired product as white crystals, mp 198°-201° C. (dec.).

Herkunft & Nachweise