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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 36145Erstellt: 24. Oktober 2026

N-heptylacetamide → 1-Heptanamine, N-ethyl-

https://huagongshe.com/de/reaction/36145

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-heptylacetamideHCID 347488—
EduktAluminium lithium hydrideHCID 21226445—
EduktSodium hydroxide--water (1/1/1)HCID 23719242—
LösungsmittelDiethyl EtherHCID 3283—
Produkt1-Heptanamine, N-ethyl-HCID 48038—

Reaktionsschritte

A mixture of a solution of 5.5 gms of the N-heptylacetamide in 150 ml of diethyl ether and 3.99 gms of lithium aluminum hydride are stirred at room temperature for 18 hours. The reaction mixture is then worked up with H2O/NaOH by the Fieser method, following which the organic layer is dried over MgSO4, filtered, and concentrated under vacuum to give N-heptyl-N-ethylamine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05412137
Quelldatensatzuspto-grants-1995_05
ORD IDord-f3528eb525984558858b648e2ac6c3f7
Quellennotizuspto-grants-1995_05