HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl benzoylacetate → N-(6-methoxybenzothiazol-2-yl)-3-oxo-3-phenylpropanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl benzoylacetate | HCID 7170 | — |
| Edukt | 2-Amino-6-methoxybenzothiazole | HCID 15630 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | N-(6-methoxybenzothiazol-2-yl)-3-oxo-3-phenylpropanamide | HCID 19975336 | — |
Reaktionsschritte
Ethyl benzoyl acetate (9.5 ml) and 2-amino-6-methoxy benzothiazole (9.01 g) are heated to 140° under house vacuum for 2 hours. After cooling, the residue is taken up in acetone and filtered. The precipitate is dissolved in hot DMF to give an amide, N-(6-methoxybenzothiazol -2-yl)-3-oxo-3-phenylpropanamide (II).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05412141 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-05a90fbe55264688b82f73bcc6384ff0 |
| Quellennotiz | uspto-grants-1995_05 |