HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Nitrophenyl chloroformate → 4-Nitrophenyl 2-(3-thiophenyl)ethyl carbonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Edukt | Thiophene-3-ethanol | HCID 83731 | — |
| Produkt | 4-Nitrophenyl 2-(3-thiophenyl)ethyl carbonate | HCID 57094331 | — |
Reaktionsschritte
Using the method of Example 7a, 3-thiopheneethanol was treated with 4-nitrophenyl chloroformate to afford, after purification by flash chromatography (EtOAc:hexane (1:9)), the title product (56%); TLC, Rf =0.25, EtOAc:hexane (1:9).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05414132 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-5c4202d739af496d99d2ebc2c9abeb12 |
| Quellennotiz | uspto-grants-1995_05 |