HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide → HCID 178418472, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide | HCID 53745902 | — |
| Edukt | Sodium hydrogen sulphide | HCID 86586439 | — |
| Produkt | HCID 178418472 | HCID 178418472 | 63,6% |
Reaktionsschritte
Using the procedure in Preparation 34, 6.4 g (0.02 mol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide was reacted with 4.8 g (0.066 mol) of sodium hydrogen sulfide to afford 4.2 g of the title compound, mp 178-180° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133270 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-7e85f89eba9e47fca091b576cd539398 |
| Quellennotiz | uspto-grants-2000_10 |