HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tris(pentafluorophenyl)borane → Tris(pentafluorophenyl)borane hydrate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tris(pentafluorophenyl)borane | HCID 582056 | — |
| Edukt | Borane, tris(pentafluorophenyl)-, trihydrate | HCID 11261567 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Tris(pentafluorophenyl)borane hydrate | HCID 15875499 | — |
Reaktionsschritte
A mixture of 0.566 gram (1 mmol) (C6F5)3B.3H2O as prepared in Example 1 and 1.024 grams (2 mmol) (C6F5)3B in 10 mL dichloromethane was stirred for 15 minutes and then evaporated to dryness under vacuum. A quantitative yield of the product remained and was stored under dry nitrogen.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05416177 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-947c77284e834395add5a41dba46ce12 |
| Quellennotiz | uspto-grants-1995_05 |