HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | N-Isopropylhydroxylamine Hydrochloride | HCID 170873 | — |
| Edukt | 2-Chloro-6-(trimethylsilyl)benzoyl chloride | HCID 15183557 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide | HCID 18630150 | — |
Reaktionsschritte
The title compound was prepared by reaction of the compound of Example b and the i-propylhydroxylamine hydrochloride in dioxane in the presence of two equivalents of triethylamine using the amination methods described above. m.p. 175-179° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-58ede89b1a4445c48b4b5908b0f6f8c5 |
| Quellennotiz | uspto-grants-2000_10 |