HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-Methylisatin → HCID 13519800, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-Methylisatin | HCID 14313 | — |
| Edukt | Bromine | HCID 24408 | — |
| Lösungsmittel | 1,1-Dichloroethane | HCID 6365 | — |
| Produkt | HCID 13519800 | HCID 13519800 | — |
Reaktionsschritte
The 7-methylisatin (16.1 g, 0.1 mole) is suspended in dichloroethane (2000 ml) and the suspension is heated and irradiated with a high intensity light source to the reflux point. Bromine (24.3 g, 0.15 mole) is added dropwise over a one hour period.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04530929 |
| Quelldatensatz | uspto-grants-1985_07 |
| ORD ID | ord-ff59d6552f17494db82c24337df43ee5 |
| Quellennotiz | uspto-grants-1985_07 |