HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(Pyridin-2-yl)propan-1-amine → HCID 178512789, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(Pyridin-2-yl)propan-1-amine | HCID 3159614 | — |
| Edukt | S-methyl isothiourea hemisulfate | HCID 6604939 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 178512789 | HCID 178512789 | — |
Reaktionsschritte
A solution of 2-(3-aminopropyl)pyridine (2.72 g) and S-methylthiouronium sulphate (2.78 g) in water (40 ml) is heated under reflux for 28 hours. The product isolated by the manner described in Example 1 was recrystallized from methanol, yielding 3-(2-pyridyl)propylguanidine sulphate, m.p. 185°-187° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04088769 |
| Quelldatensatz | uspto-grants-1978_05 |
| ORD ID | ord-7f50331ed03b4f5c90002a3e7ae7bccd |
| Quellennotiz | uspto-grants-1978_05 |