HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Glycyl-glycine benzyl ester hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Benzyl (tert-butoxycarbonyl)glycylglycinate | HCID 3244524 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | Glycyl-glycine benzyl ester hydrochloride | HCID 13996146 | — |
Reaktionsschritte
10.3 Parts N-t-butoxycarbonylglycylglycine benzyl ester is dissolved in 200 parts dioxane and treated with a 10 fold excess of 2 N hydrochloric acid in dioxane for 10 minutes. Removal of the solvent under reduced pressure affords pure glycylglycine benzyl ester hydrochloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04092304 |
| Quelldatensatz | uspto-grants-1978_05 |
| ORD ID | ord-649622d36011435d853bf41132b09046 |
| Quellennotiz | uspto-grants-1978_05 |