HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Allyl bromide → 2-(2-(Allyloxy)ethoxy)ethanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Allyl bromide | HCID 7841 | — |
| Edukt | Diethylene Glycol | HCID 8117 | — |
| Lösungsmittel | NaH THF | HCID 23694757 | — |
| Produkt | 2-(2-(Allyloxy)ethoxy)ethanol | HCID 84777 | 82% |
Reaktionsschritte
Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08524104B1 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-4e69885985a74b1ca4a5f8fc798f2882 |
| Quellennotiz | uspto-grants-2013_09 |