HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 2,2-Dimethyl-3-octenoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Water butanol | HCID 22253497 | — |
| Edukt | 2,2-Dimethyl-3-octene nitrile | HCID 86755156 | — |
| Produkt | 2,2-Dimethyl-3-octenoic acid | HCID 54196509 | — |
Reaktionsschritte
2,2-Dimethyl-3-octenoic acid is prepared by adding 2,2-dimethyl-3-octene nitrile (1.51 g, 0.01 m) to a solution prepared from 15% NaOH in butanol/H2O (2:3) (30 mL). The reaction mixture is stirred and refluxed for 7 hours, is cooled and made acidic with 10% hydrochloric acid. The reaction mixture is extracted with diethyl ether and the extract washed with saturated NaCl and dried over MgSO4, filtered and concentrated to give 2,2-dimethyl-3-octenoic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06028083 |
| Quelldatensatz | uspto-grants-2000_02 |
| ORD ID | ord-42a13ce3df6d4616a65a8adc5897f498 |
| Quellennotiz | uspto-grants-2000_02 |