HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → HCID 178418566, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 5-Isocyanato-1,2,3-trimethoxybenzene | HCID 517766 | — |
| Edukt | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride | HCID 13731126 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 178418566 | HCID 178418566 | 46,4% |
Reaktionsschritte
The procedure described in Example 2 was followed, using 2.5 g of 3,4,5-trimethoxyphenyl isocyanate, 4.4 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride, 1.2 g of triethylamine and 50 ml of methylene chloride, to give 1.6 g (23% of theory) of N-(3,4,5-trimethoxyphenyl)-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 239°-241° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04722926 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-a578f973ce364f93924ecc2ae775a857 |
| Quellennotiz | uspto-grants-1988_02 |