HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Anisoyl chloride → N3-(4-Methoxybenzoyl)-N2-[1-(4-pyridyl)-piperidin-4-ylmethyl]-2,3-pyridinediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Anisoyl chloride | HCID 7477 | — |
| Edukt | N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine | HCID 12150690 | — |
| Produkt | N3-(4-Methoxybenzoyl)-N2-[1-(4-pyridyl)-piperidin-4-ylmethyl]-2,3-pyridinediamine | HCID 9825165 | 15,1% |
Reaktionsschritte
Using a similar procedure to that described in Example 2, Part D, N2-[1-(4-pyridyl)piperidin-4-ylmethyl]-2,3-pyridinediamine (300 mg, 1.06 mmol) and 4-methoxybenzoyl chloride (200 mg, 1.17 mmol) yielded 67 mg (15%) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06610704B1 |
| Quelldatensatz | uspto-grants-2003_08 |
| ORD ID | ord-f78d822de0c34820b1a6d2279bc6f2ea |
| Quellennotiz | uspto-grants-2003_08 |