HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethylacetate heptane → 6-chloro-N-methyl-4-phenylpyridazin-3-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethylacetate heptane | HCID 21899848 | — |
| Edukt | 6-Chloro-4-phenylpyridazin-3-amine | HCID 76848713 | — |
| Produkt | 6-chloro-N-methyl-4-phenylpyridazin-3-amine | HCID 86698478 | — |
Reaktionsschritte
The title compound was prepared in analogy to example 1, intermediate a, from 6-chloro-4-phenyl-pyridazin-3-ylamine and using a gradient of n-heptane:ethyl acetate (100:0 to 40:60) for the chromatographic purification. Light yellow solid (52%). MS (ESI+): m/z=220.064 ([M+H]+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08748434B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-7e66c99393e84a34bdda062980d3e56e |
| Quellennotiz | uspto-grants-2014_06 |