HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine → 4-(4,6-Dimorpholino-1,3,5-triazin-2-yl)benzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine | HCID 224967 | — |
| Edukt | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Produkt | 4-(4,6-Dimorpholino-1,3,5-triazin-2-yl)benzonitrile | HCID 58507720 | 50% |
Reaktionsschritte
The title compound was prepared by following the procedure of example 473 step 2 using 4,4′-(6-chloro-1,3,5-triazine-2,4-diyl)dimorpholine and 4-cyanophenyl-boronic acid. Yield 86 mg, 50% yield; HPLC: Rt=2.60 min; MS 353 [M+H].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08748421B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-e8c283c2704a4069a50628c089ea924e |
| Quellennotiz | uspto-grants-2014_06 |