Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1,4-Dioxane | HCID 31275 | — |
| Edukt | 6-Chloroquinaldine | HCID 135965 | — |
| Produkt | 6-Chloroquinoline-2-carbaldehyde | HCID 271283 | — |
Reaktionsschritte
A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08530476B2 |
|---|
| Quelldatensatz | uspto-grants-2013_09 |
|---|
| ORD ID | ord-2952c511f0834aa6ab9efb4ef46915e5 |
|---|
| Quellennotiz | uspto-grants-2013_09 |
|---|
