HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triphosgene → 5-Bromo-2-isocyanatomethyl-1,3-dimethyl-benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triphosgene | HCID 94429 | — |
| Edukt | (4-Bromo-2,6-dimethylphenyl)methanamine | HCID 39872008 | — |
| Edukt | 6-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59635673 | — |
| Produkt | 5-Bromo-2-isocyanatomethyl-1,3-dimethyl-benzene | HCID 58102394 | — |
Reaktionsschritte
The title compound was prepared from 4-bromo-2,6-dimethyl-benzylamine and triphosgene following a procedure analogous to that described in Step 4 of Intermediate 1. Mass spectrum (EI): m/z=239/241 (Br) [M]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08754076B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-96f615c1fefb4223bae3942daee0a930 |
| Quellennotiz | uspto-grants-2014_06 |