Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Benzylamine | HCID 7504 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 2-Chloro-1,1-dimethoxyethane | HCID 60986 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | N-Benzyl-2,2-dimethoxyethan-1-amine | HCID 276572 | — |
Reaktionsschritte
Benzylamine (0.927 kg), chloroacetaldehydedimethylacetal (0.909 kg), sodium hydroxide solution (0.35 kg) in 2.72 L of water were charged into the flask under stirring at 25-30° C. for 10-15 min. Reaction mass was heated to 100-102° C. under stirring for 30 hrs. After completion of reaction, reaction mass was allowed to settle for 30 min. Two layers are separated and upper product layer was collected, distilled under high vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08754215B2 |
|---|
| Quelldatensatz | uspto-grants-2014_06 |
|---|
| ORD ID | ord-90d4d3a682834183b60fa6376a558089 |
|---|
| Quellennotiz | uspto-grants-2014_06 |
|---|
