Dichloromethane → HCID 86662562, Verbindung

Beteiligte Stoffe

Reaktionsschritte

Using the general procedure for synthesizing naphthyl (aminoacid ester) phosphorochloridates the tosylate salt of benzyloxy-L-alanine (1.5 g), naphthalen-1-yl phosphorodichloridate (1.10 g), TEA (1.14 mL), and DCM (20 mL) were combined to give (2S)-benzyl 2-(chloro(naphthalen-1-yloxy)-phosphorylamino)-propanoate in an 89% yield (1.53 g), as a pale yellow thick oil.

Herkunft & Nachweise