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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 41289Erstellt: 24. Oktober 2026

2,2'-Dimethyl-5,5'-bis(3-bromo-1-adamantyl)biphenyl → 2,2'-Dimethyl-5,5'-bis(3-(3,5-diethynylphenyl)-1-adamantyl)biphenyl

https://huagongshe.com/de/reaction/41289

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,2'-Dimethyl-5,5'-bis(3-bromo-1-adamantyl)biphenylHCID 67524109—
Edukt2,2'-Dimethyl-5,5'-bis(1-adamantyl)biphenylHCID 86641950—
Produkt2,2'-Dimethyl-5,5'-bis(3-(3,5-diethynylphenyl)-1-adamantyl)biphenylHCID 8664195173,5%

Reaktionsschritte

From the obtained 2,2′-dimethyl-5,5′-bis(1-adamantyl)-biphenyl 10 g, the same method as in Synthesis Example 7 was used to synthesize 2,2′-dimethyl-5,5′-bis(3-bromo-1-adamantyl)biphenyl 4.5 g, then the same method as in Synthesis Example 3 was used to obtain 2,2′-dimethyl-5,5′-bis(3-(3,5-diethynylphenyl)-1-adamantyl)biphenyl 3.8 g.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08530596B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-8af8d5cfae954018b9b767f588c5e2c4
Quellennotizuspto-grants-2013_09