HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Bromo-2,6-dimethoxybenzoic acid → HCID 13493825, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Bromo-2,6-dimethoxybenzoic acid | HCID 2774744 | — |
| Edukt | 1-(1-Propylpyrrolidin-2-yl)methanamine | HCID 12829004 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | HCID 13493825 | HCID 13493825 | 79% |
Reaktionsschritte
The title compound was prepared from 3-bromo-2,6-dimethoxybenzoic acid via the acylchloride and (-)-1-n-propyl-2-(aminomethyl)pyrrolidine in the same manner as described in Example 8. Yield 79%. M.p. 103°-104° C. [α]D20 =-85.4° (c=0.5; CHCl3).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04789683 |
| Quelldatensatz | uspto-grants-1988_12 |
| ORD ID | ord-1248cf2a2c5c4dd19b1b4117c142eab7 |
| Quellennotiz | uspto-grants-1988_12 |