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HRID 414293Erstellt: 24. Oktober 2026

Triphenylphosphine → (2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromide

https://huagongshe.com/de/reaction/414293

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriphenylphosphineHCID 11776—
EduktPentafluorobenzyl bromideHCID 74484—
LösungsmittelDiethyl EtherHCID 3283—
Produkt(2,3,4,5,6-Pentafluorophenyl)methyl-triphenyl-phosphonium;bromideHCID 21282127—

Reaktionsbedingungen

Temperatur130 °C

Reaktionsschritte

The toluene solution from Stage 1 was mixed with triphenyl phosphine (1 g) and heated at 130° C. for 3 hours. After cooling, the solution was diluted with diethyl ether (5 cm3) and the title compound filtered off, washed with hexane (4×5 cm3) and dried by suction.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04791139
Quelldatensatzuspto-grants-1988_12
ORD IDord-071913ea308748ad9b60322c80e9fd44
Quellennotizuspto-grants-1988_12