HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
8-Pentadecanamine → N-(1-heptyloctyl)-9-bromoperylene-3,4-dicarboximide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 8-Pentadecanamine | HCID 232907 | — |
| Edukt | 9-Bromoperylene-3,4-dicarboxylic anhydride | HCID 57972943 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Lösungsmittel | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Produkt | N-(1-heptyloctyl)-9-bromoperylene-3,4-dicarboximide | HCID 44139396 | — |
Reaktionsbedingungen
| Temperatur | 135 °C |
|---|
Reaktionsschritte
Under protective gas, a mixture of 3 g (7.48 mmol) of 9-bromoperylene-3,4-dicarboxylic anhydride and 8 g (35 mmol) of 1-heptyloctylamine in 150 ml of N-methylpyrrolidone and 3 ml of acetic acid was heated to 135° C. for 20 h.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08088922B2 |
| Quelldatensatz | uspto-grants-2012_01 |
| ORD ID | ord-4fc8d1b5e1ab4ae997a5638e367fb832 |
| Quellennotiz | uspto-grants-2012_01 |