HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tert-butyl malonate → HCID 178516624, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tert-butyl malonate | HCID 21883978 | — |
| Edukt | Sodium t-butoxide | HCID 23676156 | — |
| Edukt | 1-Isocyano-2-methylpropan-2-yl methyl carbonate | HCID 25267464 | — |
| Edukt | 4-(4-Cyclopropylpiperazin-1-yl)benzaldehyde | HCID 61441753 | — |
| Edukt | HCID 178507353 | HCID 178507353 | — |
| Produkt | HCID 178516624 | HCID 178516624 | — |
Reaktionsschritte
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.86 g, 6.5 mmol), 4-(4-cyclopropylpiperazin-1-yl)benzaldehyde (1.5 g, 6.5 mmol), mono-tert-butyl malonate (1.04 g, 6.5 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (1.02 g, 6.5 mmol) with stirring for 2 days and sodium tert.-butoxide (0.60 g, 5.4 mmol) according to method 5.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08530670B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-e2a645ca183440489f20f4308c019703 |
| Quellennotiz | uspto-grants-2013_09 |