HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Oxoglutaric Acid → 1,4,5,6-Tetrahydro-6-oxo-3-pyridazinecarboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Oxoglutaric Acid | HCID 51 | — |
| Edukt | Hydrazine | HCID 9321 | — |
| Produkt | 1,4,5,6-Tetrahydro-6-oxo-3-pyridazinecarboxylic acid | HCID 99621 | 99% |
Reaktionsschritte
The disclosed embodiments stem from the examination of several classes of compounds that quantitatively react with hydrazine to form stable organic products. The reaction of 2-ketoglutaric acid with hydrazine reacts to provide a greater than 99% yield of 6-oxo-1,4,5,6-tetrahydro-pyridazine-3-carboxylic acid (PCA) based on hydrazine as the limiting reagent. It has been found that this compound allows for the facile remediation of hydrazine under a variety of conditions. The focus of the disclosed embodiments concerns the use of 2-ketoglutaric acid or other dicarbonyl compounds for the remediation of hydrazine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08535430B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-e3234c6d563d46798823285107d150ba |
| Quellennotiz | uspto-grants-2013_09 |