HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetonitrile → 5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetonitrile | HCID 6342 | — |
| Edukt | 4-Fluorophenol | HCID 9732 | — |
| Edukt | 1-Methylcyclohexanol | HCID 11550 | — |
| Produkt | 5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol | HCID 57470221 | — |
Reaktionsschritte
5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol (C-13) was synthesized following the general scheme above starting from 4-fluorophenol and 1-methylcyclohexanol. Overall yield (3%). HPLC ret. time 3.00 min, 10-99% CH3CN, 5 min run; ESI-MS 224.2 m/z (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08101767B2 |
| Quelldatensatz | uspto-grants-2012_01 |
| ORD ID | ord-cac52f274a8d44cf92788386fe6d806b |
| Quellennotiz | uspto-grants-2012_01 |