HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isonicotinic Acid → Isonicotinoyl chloride hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isonicotinic Acid | HCID 5922 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
Reaktionsschritte
A solution of isonicotinic acid (0.10 g, 0.8 mmol) and thionyl chloride (1 mL) were heated to reflux for 2 h and concentrated. The product obtained was used immediately in the following step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536194B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-0d0bda2a4ecf4b5fa1825fca2cb4ad7b |
| Quellennotiz | uspto-grants-2013_09 |