HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Chloro-5-formyl-1,3-dimethyluracil → 1,3-Dimethyl-6-(methylthio)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| Edukt | Sodium methanethiolate | HCID 4378561 | — |
| Produkt | 1,3-Dimethyl-6-(methylthio)-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 86658685 | — |
Reaktionsschritte
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.404 g, 2.00 mmol) and sodium thiomethoxide (0.154 g, 2.20 mmol in 4 ml 1,4-dioxane) were used to obtain the title compound. The crude product was purified by washing with n-pentane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08536210B2 |
| Quelldatensatz | uspto-grants-2013_09 |
| ORD ID | ord-c7198cb84a3645cf8fbf9974ac7f14d0 |
| Quellennotiz | uspto-grants-2013_09 |