HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Vinylnaphthalene → HCID 15527073, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Vinylnaphthalene | HCID 13230 | — |
| Edukt | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Produkt | HCID 15527073 | HCID 15527073 | — |
Reaktionsschritte
According to GP, 2.22 mmol (=0.40 g) of 1-(4-fluorophenyl)piperazine and 2.22 mmol (=0.34 g) of 2-vinylnaphthalene are reacted with 5 mol % (=0.111 mmol=70 μl) of n-BuLi solution. Column-chromatographic separation with ethyl acetate/n-hexane (1:1) gives the product 1-(4-fluorophenyl)-4-[2-(2-naphthyl)-1-ethyl]piperazine as a light-yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06313297B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-fd5fb53121034ed39783491c1f364175 |
| Quellennotiz | uspto-grants-2001_11 |