Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 433926Erstellt: 24. Oktober 2026

3,4-Dimethoxyphenethyl alcohol → Methyl 2-Hydroxy-3-(2-(3,4-dimethoxyphenyl)ethoxy)-3,3-diphenylpropionate

https://huagongshe.com/de/reaction/433926

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3,4-Dimethoxyphenethyl alcoholHCID 81911—
EduktMethyl 3,3-diphenyloxirane-2-carboxylateHCID 10587027—
KatalysatorBoron trifluoride etherateHCID 8000—
LösungsmittelDichloromethaneHCID 6344—
ProduktMethyl 2-Hydroxy-3-(2-(3,4-dimethoxyphenyl)ethoxy)-3,3-diphenylpropionateHCID 18756198—

Reaktionsschritte

7 g (27.5 mmol) of methyl 3,3-diphenyl-2,3-epoxypropionate and 5.5 g (30.2 mmol) of 2-(3,4-dimethoxyphenyl)ethanol were dissolved in 20 ml of dichloromethane and, at room temperature, 5 drops of boron trifluoride etherate were added. The solution was stirred for 2 hours. The solvent was then distilled off, and the residue (10.7 g, 89%) was immediately reacted further.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06670367B1
Quelldatensatzuspto-grants-2003_12
ORD IDord-25a8cc06e044439baf8afa2a89b389b2
Quellennotizuspto-grants-2003_12