Hydrochloric Acid → HCID 10012985, Verbindung

HRID 435094

Reaktionsgleichung

Reaktionsgleichung von HRID 435094
[ClH:1].[CH2:2]=O.[CH2:4]([O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:5][CH2:6][CH3:7]>C1C=CC=CC=1>[CH2:4]([O:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:2][Cl:1])=[CH:11][CH:10]=1)[CH2:5][CH2:6][CH3:7]

Komponenten

5

Edukt 3

HCID 313Hydrochloric Acid2×HCID 712FormaldehydeHCID 14311Butyl phenyl ether

Produkt 1

HCID 10012985HCID 10012985, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 241BenzeneLösungsmittel

Versuchsvorschrift

Hydrogen chloride gas is passed into a mixture of 9.6 g of paraformaldehyde and 40 ml of 37% aqueous hydrochloric acid up to the formation of a clear solution. Subsequently, a solution of 30 g of n-butyloxybenzene in 20 ml of benzene is added dropwise at 15°-20° and the reaction mixture stirred for 4 hours at this temperature. The organic phase is separated off, washed twice with 30 ml amounts of water, dried and distilled. After distilling off the benzene, there is obtained 27 g of 4-n-butyloxybenzyl chloride; b.p. 102°/1 m bar.

Aufarbeitung

  1. customThe organic phase is separated off
  2. washwashed twice with 30 ml amounts of water
  3. customdried
  4. distillationdistilled
  5. distillationAfter distilling off the benzene

Quellen und Nachweise

ORD-Eintrag
ord-7310df565a0349a793d7b615a7027a80
Quelldatensatz
uspto-grants-1983_08
Patentnummer
US04400293

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