HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Azide → 3-Aminorifamycin S
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Azide | HCID 33557 | — |
| Edukt | Rifamycin S | HCID 6436726 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 3-Aminorifamycin S | HCID 12889622 | 25,5% |
Reaktionsschritte
50 g rifamycin S were dissolved in 200 ml dimethyl formamide and added with 9 g sodium azide. After 36 hours at a temperature of +5° C, the reaction mixture was treated as in Example 3, to obtain 13 g 3-amino-rifamycin S identical to that described in Example 3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04007169 |
| Quelldatensatz | uspto-grants-1977_02 |
| ORD ID | ord-f05fa6bfaf3840458238356cf61f0acd |
| Quellennotiz | uspto-grants-1977_02 |