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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 436368Erstellt: 24. Oktober 2026

Acetic Acid → 1-Methyl-s-triazolo[4,3-a]quinoxaline

https://huagongshe.com/de/reaction/436368

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetic AcidHCID 176—
Edukt2-HydrazinoquinoxalineHCID 289847—
Produkt1-Methyl-s-triazolo[4,3-a]quinoxalineHCID 21817404—

Reaktionsschritte

A 5 g. portion of 2-hydrazinoquinoxaline was stirred at reflux temperature in acetic acid for 3 hours. The reaction mixture was then cooled, and was evaporated to dryness under vacuum. The product was found to melt at 210°-12° C. without purification, and was identified as 1-methyl-s-triazolo[ 4,3-a]quinoxaline by NMR analysis and elemental microanalysis, the results of which follow.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04008322
Quelldatensatzuspto-grants-1977_02
ORD IDord-4a363311389b443a82fd6b09271767e6
Quellennotizuspto-grants-1977_02