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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 436634Erstellt: 24. Oktober 2026

Potassium Hydroxide → HCID 21452919, Verbindung

https://huagongshe.com/de/reaction/436634

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium HydroxideHCID 14797—
Edukt1,7-HeptanediamineHCID 69533—
Edukt4-Isopropoxybenzoyl chlorideHCID 2724465—
Lösungsmittel1,2-DichloroethaneHCID 11—
ProduktHCID 21452919HCID 21452919—

Reaktionsschritte

m.p. 135°-136° C., 10.9 g., was prepared as in Example 1 using a solution of 4-isopropoxybenzoyl chloride (from 18.0 g. of 4-isopropoxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 8.9 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04009208
Quelldatensatzuspto-grants-1977_02
ORD IDord-91a8fc79e8c046b988e192deb662d36c
Quellennotizuspto-grants-1977_02