HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-bis(3-aminopropyl)methylamine → HCID 21428657, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-bis(3-aminopropyl)methylamine | HCID 7777 | — |
| Edukt | Homophthalic anhydride | HCID 12801 | — |
| Produkt | HCID 21428657 | HCID 21428657 | — |
Reaktionsschritte
N,N-Bis-[3-(3,4-dihydro-1,3-dioxo-2-(1H)-isoquinolyl)-propyl]-methylamine was prepared analogous to Example 30 from 15 gm of isochroman-1,3-dione and N,N-bis-(3-amino-propyl)-methylamine. The hydrochloride was precipitated from acetone with ethereal hydrochloric acid and recrystallized from ethanol. M.p. of the hydrochloride: 202° -205° C; yield: 13.8 gm (32% of theory).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04031219 |
| Quelldatensatz | uspto-grants-1977_06 |
| ORD ID | ord-83a873ba39c44c5999d3ab0d88e33056 |
| Quellennotiz | uspto-grants-1977_06 |