HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-[(4-Chlorophenyl)methylidene]-2,2-dimethylcyclopentan-1-one → 5-(4-Chlorobenzyl)-2,2-dimethylcyclopentanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-[(4-Chlorophenyl)methylidene]-2,2-dimethylcyclopentan-1-one | HCID 53421021 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 5-(4-Chlorobenzyl)-2,2-dimethylcyclopentanone | HCID 11424896 | — |
Reaktionsschritte
5 g of 2-(4-chlorobenzylidene)-5,5-dimethylcylopentanone (prepared in Example 5) was dissolved in 40 ml of ethanol, and 60 mg palladium-carbon (10%) was added to the mixture. The hydrogenation reaction was carried out under normal pressure until theoretical amount of hydrogen was absorbed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05519160 |
| Quelldatensatz | uspto-grants-1996_05 |
| ORD ID | ord-374bf906581b40649dcba35c765543d2 |
| Quellennotiz | uspto-grants-1996_05 |