HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → p-Chloromethylphenylacetyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 4-(Chloromethyl)phenylacetic acid | HCID 10313419 | — |
| Produkt | p-Chloromethylphenylacetyl chloride | HCID 20380233 | — |
Reaktionsschritte
A mixture of 1 g of p-chloromethylphenylacetic acid and 6 ml of thionyl chloride is stirred at room temperature for 25 hours after which the excess thionyl chloride is removed under vacuum to yield p-chloromethylphenylacetyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04045438 |
| Quelldatensatz | uspto-grants-1977_08 |
| ORD ID | ord-05a6d14492d4416e891aa8b6f6a8d12a |
| Quellennotiz | uspto-grants-1977_08 |