HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bisphenol A → 1,1,3,3-Tetramethylindan-5-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bisphenol A | HCID 6623 | — |
| Edukt | 4-tert-Butylphenol | HCID 7393 | — |
| Produkt | 1,1,3,3-Tetramethylindan-5-ol | HCID 104567 | 35,2% |
Reaktionsschritte
172 g (1.15 mol) of 4-tert.-butylphenol, 57.5 g (0.25 mol) of 2,2-bis-(4-hydroxyphenyl)-propane and 20 g of an ion exchanger are heated with stirring for 5 hours to about 170° C. in an autoclave. The ion exchanger is then filtered off while still hot, leaving 208.5 g of a reaction mixture from which 16.7 g (0.088 mol) of 5-hydroxy-1,1,3,3-tetramethyl indane are isolated by fractional distillation.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04045499 |
| Quelldatensatz | uspto-grants-1977_08 |
| ORD ID | ord-3f2b2490071144eca1e794d8786ab515 |
| Quellennotiz | uspto-grants-1977_08 |