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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 443366Erstellt: 24. Oktober 2026

Ethyl Acetate → (2E,6E)-2-[(3E)-4,8-Dimethylnona-3,7-dien-1-YL]-6-methylocta-2,6-diene-1,8-diol

https://huagongshe.com/de/reaction/443366

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl AcetateHCID 8857—
EduktAluminiumhydrideHCID 21584524—
EduktHCID 53654873HCID 53654873—
LösungsmittelDiethyl EtherHCID 3283—
Produkt(2E,6E)-2-[(3E)-4,8-Dimethylnona-3,7-dien-1-YL]-6-methylocta-2,6-diene-1,8-diolHCID 6373042—

Reaktionsschritte

The ester thus obtained was further reduced by aluminum hydride (prepared from 760 mg of lithium aluminum hydride and 880 mg of aluminum chloride) in 7 ml of ether. After completion of the reaction, ethyl acetate was added to the reaction mixture, and the precipitate was filtered off. The filtrate was evaporated to dryness, yielding 3.5 g of the desired product.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04260551
Quelldatensatzuspto-grants-1981_04
ORD IDord-6417daee1ff942c6842215cc7af87313
Quellennotizuspto-grants-1981_04