HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
[1-(4-fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol → 1-(4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | [1-(4-fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol | HCID 67303957 | — |
| Katalysator | Manganese | HCID 23930 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 1-(4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde | HCID 85997993 | — |
Reaktionsschritte
[1-(4-Fluoro-phenyl)-2-methyl-1H-imidazol-4-yl]-methanol is dissolved in methylene chloride. Mangan (IV) oxide is added and the reaction mixture is stirred at room temperature for 3 days. The suspension is filtered through a dicalite speed plus pad and the desired compound (4-fluoro-phenyl)-2-methyl-1H-imidazole-4-carbaldehyde is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08481548B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-687063cbc1674a448e4a228f4346c316 |
| Quellennotiz | uspto-grants-2013_07 |