HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Fluorophenethyl Alcohol → N-{4-[2-(4-Fluorophenyl)ethoxy]benzoyl}glycine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Fluorophenethyl Alcohol | HCID 82068 | — |
| Edukt | N-(4-Hydroxybenzoyl)glycine tert-butyl ester | HCID 10682169 | — |
| Produkt | N-{4-[2-(4-Fluorophenyl)ethoxy]benzoyl}glycine | HCID 66812288 | 91% |
Reaktionsschritte
The same reaction as in Example 1 (1b) was conducted using N-(4-hydroxybenzoyl)glycine tert-butyl ester (249 mg, 0.991 mmol) prepared in Example 1 (1a) and 2-(4-fluorophenyl)ethanol (150 μL, 1.20 mmol) to give 241 mg of the title compound (yield: 91%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08497397B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-6afa8e6ef7d241f0aba772375422b751 |
| Quellennotiz | uspto-grants-2013_07 |