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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 460500Erstellt: 24. Oktober 2026

Phenol → 4,4,4'4'-Tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexene

https://huagongshe.com/de/reaction/460500

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPhenolHCID 996—
Edukt2-IsopropylphenolHCID 6943—
Edukt(1,1'-Bicyclohexyl)-4-oneHCID 41690—
LösungsmittelMethanolHCID 887—
Produkt4,4,4'4'-Tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexeneHCID 18446146232,7%

Reaktionsschritte

The same method as specified in Reference Example 1 was used, except that 236.8 g of 0-isopropyl phenol and 23.7 g of methanol were used instead of 209.4 g of phenol and 18.9 g of methanol, and that a solution made of 39.0 g of 4,4′-bicyclohexanon and 39.0 g of 0-isopropyl phenol dissolved in 15.8 g of methanol was used instead of a solution made of 24.2 g of 4,4′-bicyclohexanon and 24.2 g of phenol dissolved in 24.2 g of methanol, to achieve reaction, neutralization, crystallization and filtering to obtain 175.9 g of 4,4,4′4′-tetra(3-isopropyl-4-hydroxyphenyl)bicyclohexene as white solid (still wet with the solution).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07196232B2
Quelldatensatzuspto-grants-2007_03
ORD IDord-615c9b1d0f7a4ec4b34e754003081310
Quellennotizuspto-grants-2007_03