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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 461520Erstellt: 24. Oktober 2026

Potassium Carbonate → 4-(m-Benzoylphenyl)-2-butanone

https://huagongshe.com/de/reaction/461520

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
EduktAcetylacetoneHCID 31261—
Edukt3-(Bromomethyl)benzophenoneHCID 89586—
LösungsmittelEthanolHCID 702—
Produkt4-(m-Benzoylphenyl)-2-butanoneHCID 2049604039,7%

Reaktionsschritte

A mixture of 3-bromomethylbenzophenone (2.75 g.), acetylacetone (1 g.), potassium carbonate (1.4 g.) and ethanol (50 ml) was refluxed for 2 hours. The solvent was then evaporated and the residue extracted with ether. Distillation of the concentrated extracts gave 4-(m-benzoylphenyl)-2-butanone (1 g.), b.p. 220° C (4 mm). [An alternative preparation of this compound appears in German Offenlegungsschrift No. 2,243,444].

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04062978
Quelldatensatzuspto-grants-1977_12
ORD IDord-f75ab447997a45649acb9e00944ff338
Quellennotizuspto-grants-1977_12