HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Piperazine → 2-[2-(1-Piperazinyl)-5-thiadiazolyl]-1-methyl-5-nitroimidazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Piperazine | HCID 4837 | — |
| Edukt | Piperidine | HCID 8082 | — |
| Edukt | 2-(2-Piperidino-5-thiadiazolyl)-1-methyl-5-nitroimidazole | HCID 21390837 | — |
| Produkt | 2-[2-(1-Piperazinyl)-5-thiadiazolyl]-1-methyl-5-nitroimidazole | HCID 21390830 | — |
Reaktionsschritte
The preparation of the subject compound is carried out essentially as described for the 2-piperidino derivative (Example 28), two equivalents of piperazine replacing the piperidine. The crude project is recrystallized from 2-methoxyethanol to yield the pure compound melting at 240°-241° C. ;cl EXAMPLE 24
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04065567 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-12914646f91d4db4b530caf5515c91e9 |
| Quellennotiz | uspto-grants-1977_12 |