HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Butanol → HCID 178454803, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Butanol | HCID 263 | — |
| Edukt | Water | HCID 962 | — |
| Edukt | HCID 178476830 | HCID 178476830 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | HCID 178454803 | HCID 178454803 | 81,6% |
Reaktionsschritte
A solution of α-hydroxyethylphosphinic acid (2.2 g) and 1-butanol (5.0 g) in benzene (30 ml) was heated for 3 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 2.71 g (81.6%) of n-butyl α-hydroxyethylphosphinate (Compound No. 5).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04544652 |
| Quelldatensatz | uspto-grants-1985_10 |
| ORD ID | ord-1d8432d027704c71b7d7c4dea8657e9c |
| Quellennotiz | uspto-grants-1985_10 |