Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Chloroacetonitrile | HCID 7856 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | 1-Heptanamine, N-ethyl- | HCID 48038 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 20225324 | HCID 20225324 | — |
Reaktionsschritte
Combine 7.95 g (0.055 moles) ethyl(heptyl)amine, 3.5 ml (0.055 moles) chloroacetonitrile, 5.8 g (0.055 moles) sodium carbonate and 25 ml toluene in a sealed pressure tube. Heat to 125° C. for 18 hrs. Follow the progress of the reaction by thin layer chromatography on silica gel (CH3CN+MeOH+NH4OH, 85+10+5). At the completion of the reaction, filter the reaction mixture and evaporate the solvents to provide the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04544654 |
|---|
| Quelldatensatz | uspto-grants-1985_10 |
|---|
| ORD ID | ord-848d384f4a9e4071b0ce402d368bbeaf |
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| Quellennotiz | uspto-grants-1985_10 |
|---|
